unprotection of groups

kzhao at BIOVX1.BIOLOGY.UCLA.EDU kzhao at BIOVX1.BIOLOGY.UCLA.EDU
Sun May 25 17:55:01 EST 1997


For Sunny's question of unprotection of glucuronide:

Dissolve your compound in methanol (cold), flux ammonia for 1hr during stirring,
 and store in a refrigerator o/n.  Acetate is recovered by filtration.  See
J. Histochem. Cytochem. 2: 209-229, 1954 for details on similar compound.

Good luck,

Ke-Wei Zhao, Ph.D.
Dept. Biol. Chem.
UCLA School of Medicine
Los Angeles, CA 90095 



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