ESI fragmentation of oligosaccharides

Paul McJarrow Paul.McJarrow at nzdri.org.nz
Tue Mar 20 22:33:43 EST 2001


Dear Wilaiwan,

Try papers by Vern Reinhold, Anne Dell or Jane Thomas-Oates for a start. I've put a couple of papers at the bottom to start with. Any of the ES MSMS fragmentations will apply to the ESI-TOF but the TOF will allow greater sensitivity and less sample usage. Hope this is of help to set you on the way.
P
 aul



Lemoine J., Fournet B., Despeyroux D., Jennings K.R.,Rosenberg R. and de Hoffman E. Collision induced dissociation of alkali metal cationized and permethylated oligosaccharides: Influence of the collision energy and of the collision gas for the assignment of linkage position.Journal of the American Society for Mass Spectromtry (1993) 4, 197-203

Dell A. (1990) Preparation and desorption mass spectrometry of permethyl and peracetyl derivatives of oligosaccharides. Methods in Enzymology, 193, 647-660

Reinhold V.N., Reinhold B.B. and Chan S. (1996). Carbohydrate sequence analysis by electrospray ionization-mass spectrometry. Methods in Enzymology  271, 377-400

Paul McJarrow
Scientist
MN Section
New Zealand Dairy Research Institute
Palmerston North
New Zealand
Ph (06) 350 4600 ext 7418
Fax (06)356 1476
paul.mcjarrow at nzdri.org.nz



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