help about equilibrate phenol

Bethune international peace hospital genet at PUBLIC.SJ.HE.CN
Mon Nov 2 21:51:08 EST 1998

 How to equilibrate phenol to a PH>7.8?
    We have equilibrate phenol for one week with Tris.Cl(1M,PH8.0),
but the PH of penol phase is still under 7.0  and much phenol lose.
            thank you for help 
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