SCALEPACK questions (2)
diane h peapus
diane at kuchem.kyoto-u.ac.jp
Tue Oct 14 01:19:22 EST 1997
Greetings:
I'm scaling data sets from multiple crystals using
SCALEPACK and have a few questions that I can't find
answers to in the manual.
***********************************************************
******************* QUESTION #1) **************************
***********************************************************
I keep getting multiple error messages on every cycle
of postrefinement that say.....
___________________________________________________________
Parameter# 14 cannot be fitted
Parameter# 15 cannot be fitted
(many more of the same deleted)
Parameter# 95 cannot be fitted
___________________________________________________________
Where the parameter# ranges from 14 to 95. I
can't find anywhere that these parameters are defined
and I can't find any indication of the meaning of this
type or error. Can anyone help me out?
***********************************************************
******************* QUESTION #2) **************************
***********************************************************
In the list of IP's and reflection counts, each record
has a term that says 'no o' which could possibly be 'no
origin'? In DENZO I _didn't_ give the command 'use origin'
so many 'no o' means 'no origin.' Does anyone know if this
is true? Is the 'no o' nothing I should worry about? Or
is it an indication of error?
___________________________________________________________
1 2 3 4 5 6 7 8
IP fitted, no o 10 0.8683 -0.98 38 0 31 4 0 0 3970 3640
IP fitted, no o 11 0.8667 -0.53 48 0 36 3 0 0 3762 3582
___________________________________________________________
thanks
diane h peapus
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